WP21 Sample environment


Objectives
The principle aim of the JRA is to enhance the capabilities of sample environment available at neutron facilities. We will extend the supported sample environment at the participating facilities and provide knowledge and expertise to the collaborating participants. The three key areas of endeavour are high pressure gas cells, ultra high temperature furnaces and gas handling systems.



Have a look to the W21 Tasks section for complementary information!
Click to enlarge the pictures
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High pressure gas cells:
Significant increase in accessible pressures, both inert gas and hydrogen
Inert gases:
Report – current technology
Cells: 8 kbar, 10 kbar prototype
Gas handling systems
Cryogenic test system

Hydrogen gas handling and pressure cells:
Report – hydrogen-safe materials
Cells: 4, 6 and 8 kbar
Gas handling and other equipment
Test regimes and safety issues

Ultra high temperature furnaces:
Increase sample size, stabilisation and allow the possibility of crystal growth
In-situ measurement of conductivity and magnetic susceptibility
Make these systems more accessible and user friendly.

Objective:
to build compact furnaces optimised for neutron scattering instruments and reaching 3000K (2000K today)
• Containerless technics avoiding contamination
- Aerodynamic levitation
- Electromagnetic levitation (liquid metals), adapted to dielectric materials with electrostatic levitation technique


Gas absorption systems:
Mobile systems with user friendly integrated control systems
Extension of pressure range and temperatures 1.5k – 600k and up

Automated gas dosing systems:
Volumetric: T < 300 K, P < 1.5 bar
Volumetric and Continuous Flow: 500 K, 300 bar
Vapour Mixing System 35bar with rest-gas analysis

Gravimetric gas adsorption environment:
Build high temperature neutron environment for magnetic suspension balance 500 K, 300 bar
Build low temperature option for magnetic suspension balance 20 K, 1.5 bar




Coordinator: Zoe Bowden

Forum: WP21 Sample environment FORUM
(restricted access to JRA Partners)

Administration of the JRAWP21 Website: WP21Admin
(Access restricted)



Last modified on 27/04/2010
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